preconcentration

Determination of thymol with micellar extraction preconcentration

Authors: Tsygulyova E. I., Doronin S. Y.

For the efficient preconcentration of azo compounds – products of the interaction of 4-nitrophenyldiazonium with thymol, a system 4-nitroaniline (4-NA) – NO2 - – Triton X-100 – NaOH – ethanol has been proposed. The optimal conditions for the formation of micellarsaturated phases of the system under study have been established: 3. 10-4 M 4-NA – 3. 10-4 M NO2 - – 5% Triton X-100 – 2.8 M NaOH – 10 vol. % С2Н5ОН. A spectrophotometric study of the above system has been carried out.

Preconcentration of Е110 and Е124 Food Azodyes on Magnetite Nanoparticles Modified by CTAB

Authors: Kazimirova K. O., Khabibullin V. R., Reshetnikova I. S., Egunova O. R., Shtykov S. N.

Synthetic azodyes are widely used in paint, textile, plastic, and food, beverage, and leather, cosmetic, pharmaceutical and paper industries to make products more visually attractive to consumers. Therefore, they are also the components of waste waters and should be removed due to their potential risk to human health. Many techniques have been employed to eliminate dyes from waste water and do to preconcen- tration before analysis in food or beverage objects. One of the most popular and effective is magnetic solid-phase extraction (MSPE) with the use of magnetic nanoparticles (MNP).